A new cell for X-ray absorption spectroscopy study under high pressure
X-ray absorption fine structure (XAFS) spectroscopy is a powerful technique for the investigation of the local environment around selected atoms in condensed matter. XAFS under pressure is an important method for the synchrotron source. We design a cell for a high pressure XAFS experiment. Sintered boron carbide is used as the anvils of this high pressure cell in order to obtain a full XAFS spectrum free from diffraction peaks. In addition, a hydraulic pump was adopted to make in-suit pressure modulation. High quality XAFS spectra of ZrH2 under high pressure (up to 13 Gpa) were obtained by this cell.
作 者: ZHENG Li-Rong CHE Rong-Zheng LIU Jing DU Yong-Hua ZHOU Ying-Li HU Tian-Dou 作者单位: ZHENG Li-Rong(Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China;Graduate University of Chinese Academy of Sciences, Beijing 100049, China)CHE Rong-Zheng,LIU Jing,DU Yong-Hua,ZHOU Ying-Li,HU Tian-Dou(Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China)
刊 名: 中国物理C(英文版) ISTIC 英文刊名: CHINESE PHYSICS C 年,卷(期): 2009 33(8) 分类号: O4 关键词: high pressure XAFS boron carbide